Organic Chemistry lab

Eight 20.0 mmol of isopentyl alcohol into a 10 ml improve bottom flask match magnetic stir immobilise Add 2.3 ml of glacial acetic corrosive thusly stir the mixutre Add .15 ml of concentrated sulfuric acid Connect a peeing cooled condenser to the chemical reception flask figure out on the alter weewee and heat Reduce the heating rate if the reflux family rises to at heart 2cm of the top of the condenser When the reaction time is up issue the reaction mixture to cool to nearly room temperature. fold off the cooling water and remove the condenser with a few drops of water Transfer the reaction mixture to a love cap separator tube and add 6 ml of later using some of the after for the remove Ash the reaction mix with the after and remove cautiously Pressure may build up in the caped centrifuge tube During the first washables stir the layers until gas growth subsides before you cap the centrifuge tube and vent it much Try to remove all of the sedimen tary layer after the last washing to minimize the hail of water in the product Dry the crude isopentyl acetate by adding a small amount of anhydrous sodium sulfate carefully transfer the liquifiable to a dry 5ml conical ampule using a dry filter tip pipette Try not to transfer any drying agent with the liquid M.W b.p d solubility Acetic acid 60.1 118 1.049 compatible Isopentyl alcohol 88.1 130 0.815 2.7 Isopentyl acetate 130.2 142 0.876 0.25 sulphuric acid 98.1 290 1.84 miscibleIf you extremity to get a full essay, revise it on our website: OrderEssay.net

If you want to get a full inform ation about our service, visit our page: write my essay